Sürdürülebilir Kalkınma Amaçları

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• DüzeltmeAçık Erişim2026Scopus SJRQ2/r/kostu/10478
  Retraction Note: Synthesis of Bimetallic Nickel-Cobalt Nanoparticles Supported by Functional Multi-Walled Carbon Nanotubes by Chemical Methods: Characterization and Hydrogen Energy Generation (Topics in Catalysis, (2024), 67, 9-12, (606-614), 10.1007/s11244-024-01907-x)

  Zare, Najmeh; Karimi, Fatemeh; Altuner, Elif Esra; Mashkoor, Hussein; Tiri, Rima Nour Elhouda; Gulbagca, Fulya; Bijad, Majede; Cherif, Ali; Sen, Fatih

  The Editors-in-Chief have retracted this article because of errors and inconsistencies which raise concerns regarding the validity of the research reported in this work. A review conducted by the journal found that: The turnover frequency reported in the section entitled Catalytic Studies of Hydrogen Production was incorrectly calculated; There is no conclusive evidence that bimetallic Nickel-Cobalt nanoparticles associated with carbon nanotubes were synthesized, as the reported XRD pattern and TEM micrographs don’t support this result. Furthermore, the description of the synthesis procedure was considered to be lacking in substance; The differences between the average sizes of nanoparticles is not adequately explained. The authors were asked to comment on these concerns, but their explanation was deemed unsatisfactory. The Editors-in-Chief no longer have confidence in the research presented in this article. The authors disagree with this retraction.

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• MakaleYalnız künye2024Scopus SJRQ2/r/kostu/10531
  Synthesis of Bimetallic Nickel-Cobalt Nanoparticles Supported by Functional Multi-Walled Carbon Nanotubes by Chemical Methods: Characterization and Hydrogen Energy Generation

  Zare, Najmeh; Karimi, Fatemeh; Altuner, Elif Esra; Mashkoor, Hussein; Tiri, Rima Nour Elhouda; Gulbagca, Fulya; Bijad, Majede; Cherif, Ali; Sen, Fatih

  In this study, nickel-cobalt@functionalized multi-walled carbon nanoparticles (NiCo@f-MWCNT NPs) were synthesized, analysed, and used for hydrogen generation via methanolysis on NaBH4. For the NPs synthesis, two steps were conducted (i.e., i: MWCNT was functionalized in an acid medium to support NPs (f-MWCNT); ii: NiCo NPs were synthesized and supplemented with f-MWCNT). Various characterization techniques were used to examine the morphological structure of NiCo@f-MWCNT NPs. The transmission electron microscope (TEM) results showed that the NPs were sized as 3.941 ± 1.094 nm with a spherical structure. The X-ray diffraction analysis (XRD) results indicated an average crystalline size of 1.46 nm. The evaluation of the catalytic performance for hydrogen production revealed that the turnover frequency (TOF) was calculated to be 2934.4 min− 1 with activation energy (Ea) and enthalpy (∆H) of 39.29 kJ/mol and 36.74 kJ/mol, respectively, which indicates high viability for hydrogen transport and generation application and processes.

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